
ROSIN |
Rosin is a brittle, faintly aromatic solid, which may be transparent or slightly
translucent and possesses a glassy fracture. It is insoluble in water, but soluble in many organic solvents including alcohols,
ethers and esters, and aliphatic, aromatic and chlorinated hydrocarbons.
Resin acid composition (%) of Pinus roxburghii rosin |
S.NO |
COMPONENT |
MEAN |
RANGE |
1. |
Isopimaric |
20.9 |
19.5 – 23.1 |
2. |
Dihydroabietic |
1.5 |
1.3 – 2.5 |
3. |
Abietic |
37.5 |
35.5 – 39.4 |
4. |
Neoabietic |
15.1 |
14.2 – 15.8 |
5. |
Piamaric |
8.3 |
7.0 - 8.8 |
6. |
Levopimaric/palustric |
13.5 |
11.2 – 15.7 |
All rosin is purchased on a colour basis, which varies from pale amber to black. The lighter the colour, the more valuable
the rosin.
The procedure
for sample and colour grading is fairly simple: a portion of rosin is formed into a cube of 7/8 inch(22mm) sides. This cube
is placed inside the cabin of Lovibond Tintometer and Standard Colour of the specific grade is compared with that of the cube.
The standard colour is obtained by combination of glass slides of different shades of Red, Blue and Yellow . This is as per the procedure laid down in IS 553:1984.
SPECIFICATIONS FOR GUM ROSIN |
X |
S. No. |
Characteristic |
BIS Requirement for type Extra Pale |
Rosin Sample of R & T Factory, Nahan Extra
Pale |
1 |
Grade |
X |
X |
2 |
Colour Value (Lovibond) (Red/Yellow) |
1.35,13.0 |
1.35,13.0 |
3 |
Softening point, 0C. Min. |
70 |
72 -75 |
4 |
Relative density 270/270C |
1.050 To 1.080 |
1.061-1.065 |
5 |
Acid Number, Min. |
160 |
165-173 |
6 |
Saponification Number, Minimum |
165 |
170-183 |
7 |
Volatile matter percent by mass, Max |
1.5 |
0.365-1.000 |
8 |
Ash content, percent by mass Max |
0.05 |
0.02 -0.04 |
9 |
Matter insolvable in toluene,
percent by mass,Max |
0.10 |
0.04 -0.08 |
10 |
Unsponifiable matter, percent
by mass, Max |
6 |
2.5 - 5 |
WW |
S. No. |
Characteristic |
BIS Requirement for type Pale |
Rosin Sample of R & T Factory, Nahan Pale |
1 |
Grade |
WW |
WW |
2 |
Colour Value (Lovibond) (Red/Yellow) |
1.85,19.5 |
1.85,19.5 |
3 |
Softening point, 0C. Min. |
70 |
72 - 75 |
4 |
Relative density 270/270C |
1.0520 to 1.0820 |
1.061-1.072 |
5 |
Acid Number, Min. |
155 |
165-171 |
6 |
Saponification Number, Minimum |
160 |
170-183 |
7 |
Volatile matter percent by mass,
Max |
2.0 |
0.380-1.2000 |
8 |
Ash content, percent by mass
Max |
0.2 |
0.03-0.10 |
9 |
Matter insolvable in toluene,
percent by mass,Max |
0.40 |
0.06 -0.20 |
10 |
Unsponifiable matter, percent
by mass, Max |
6 |
2.5 - 5 |
| |
WG |
S. No. |
Characteristic |
BIS Requirement for type Pale |
Rosin Sample of R & T Factory, Nahan Pale |
1 |
Grade |
WG |
WG |
2 |
Colour Value (Lovibond) (Red/Yellow) |
2.6,30 |
2.6,30 |
3 |
Softening point, 0C. Min. |
70 |
72 -74 |
4 |
Relative density 270/270C |
1.0520 to 1.0820 |
1.065-1.075 |
5 |
Acid Number, Min. |
155 |
162-170 |
6 |
Saponification Number, Minimum |
160 |
170-180 |
7 |
Volatile matter percent by mass,
Max |
2.0 |
0.400-1.2000 |
8 |
Ash content, percent by mass
Max |
0.2 |
0.03-0.10 |
9 |
Matter insolvable in toluene,
percent by mass,Max |
0.40 |
0.06 -0.20 |
10 |
Unsponifiable matter, percent
by mass, Max |
6 |
3 - 5.2 |
| |
N |
S. No. |
Characteristic |
BIS Requirement for type Pale |
Rosin Sample of R & T Factory, Nahan Pale |
1 |
Grade |
N |
N |
2 |
Colour Value (Lovibond) (Red/Yellow) |
3.6,41 |
3.6,41 |
3 |
Softening point, 0C. Min. |
70 |
72 -74 |
4 |
Relative density 270/270C |
1.0520 to 1.0820 |
1.065-1.075 |
5 |
Acid Number, Min. |
155 |
162-170 |
6 |
Saponification Number, Minimum |
160 |
165-175 |
7 |
Volatile matter percent by mass,
Max |
2.0 |
0.500-1.2000 |
8 |
Ash content, percent by mass
Max |
0.2 |
0.05-0.10 |
9 |
Matter insolvable in toluene,
percent by mass,Max |
0.40 |
0.10 - 0.20 |
10 |
Unsponifiable matter, percent
by mass, Max |
6 |
3 - 5.2 |
| |
M |
S. No. |
Characteristic |
BIS Requirement for type Medium |
Rosin Sample of R & T Factory, Nahan Medium |
1 |
Grade |
M |
M |
2 |
Colour Value (Lovibond) (Red/Yellow) |
4.9,51 |
4.9,51 |
3 |
Softening point, 0C. Min. |
70 |
72 -74 |
4 |
Relative density 270/270C |
1.0520 to 1.0820 |
1.065-1.080 |
5 |
Acid Number, Min. |
155 |
160-165 |
6 |
Saponification Number, Minimum |
160 |
162-170 |
7 |
Volatile matter percent by mass,
Max |
2.0 |
0.700-1.000 |
8 |
Ash content, percent by mass
Max |
0.2 |
0.05-0.10 |
9 |
Matter insolvable in toluene,
percent by mass,Max |
0.40 |
0.10 -0.20 |
10 |
Unsponifiable matter, percent
by mass, Max |
6 |
3 - 5.5 |
| |
1)
The rosin is obtained from Pinus roxburghii ( Chir pine). |
2)
The rosin is obtained by Olustee Process |
3)
The testing has been done by the process defined as per IS:553:1984( except B Grade) |
4)
The product ( except X and B Grade) has been BIS certified vide licence no. 9099801 |
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SPECIFICATIONS FOR GUM ROSIN | |
K |
S. No. |
Characteristic |
BIS Requirement for type Medium |
Rosin Sample of R & T Factory, Nahan Medium |
1 |
Grade |
K |
K |
2 |
Colour Value (Lovibond) (Red/Yellow) |
6.2,60 |
6.2,60 |
3 |
Softening point, 0C. Min. |
70 |
72 -74 |
4 |
Relative density 270/270C |
1.0520 to 1.0820 |
1.065-1.080 |
5 |
Acid Number, Min. |
155 |
160-165 |
6 |
Saponification Number, Minimum |
160 |
160-170 |
7 |
Volatile matter percent by mass,
Max |
2.0 |
0.8-1.000 |
8 |
Ash content, percent by mass
Max |
0.2 |
0.05 -0.10 |
9 |
Matter insolvable in toluene,
percent by mass,Max |
0.40 |
0.10 -0.25 |
10 |
Unsponifiable matter, percent
by mass, Max |
6 |
3.5 - 5.5 |
| |
H |
S. No. |
Characteristic |
BIS Requirement for type Medium |
Rosin Sample of R & T Factory, Nahan Medium |
1 |
Grade |
H |
H |
2 |
Colour Value (Lovibond) (Red/Yellow) |
12,100 |
12,100 |
3 |
Softening point, 0C. Min. |
70 |
71 -75 |
4 |
Relative density 270/270C |
1.0520 to 1.0820 |
1.065-1.080 |
5 |
Acid Number, Min. |
155 |
160-165 |
6 |
Saponification Number, Minimum |
160 |
160-165 |
7 |
Volatile matter percent by mass,
Max |
2.0 |
1.0-1.5000 |
8 |
Ash content, percent by mass
Max |
0.2 |
0.05 -0.15 |
9 |
Matter insolvable in toluene,
percent by mass,Max |
0.40 |
0.10 -0.30 |
10 |
Unsponifiable matter, percent by mass, Max |
6 |
3.5 - 5.5 |
| |
D |
S. No. |
Characteristic |
BIS Requirement for type Dark |
Rosin Sample of R & T Factory, Nahan Dark |
1 |
Grade |
D |
D |
2 |
Colour Value (Lovibond) (Red,Yellow,Blue) |
75,160,3.0 |
75,160,3.0 |
3 |
Softening point, 0C. Min. |
70 |
72-76 |
4 |
Relative density 270/270C |
1.0520 to 1.1020 |
1.072-1.080 |
5 |
Acid Number, Min. |
155 |
157-162 |
6 |
Saponification Number, Minimum |
160 |
160-165 |
7 |
Volatile matter percent by mass,
Max |
2.0 |
1.0-1.5000 |
8 |
Ash content, percent by mass
Max |
0.5 |
0.10 - 0.40 |
9 |
Matter insolvable in toluene,
percent by mass,Max |
1.00 |
0.20 -0.80 |
10 |
Unsponifiable matter, percent
by mass, Max |
6 |
4 - 5.5 |
| |
B |
S. No. |
Characteristic |
No BIS Requirement for type Dark |
Rosin Sample of R & T Factory, Nahan Dark |
1 |
Grade |
B |
B |
2 |
Colour Value (Lovibond) |
No BIS Requirement for type |
Nil |
3 |
Softening point, 0C. Min. |
72-80 |
4 |
Relative density 270/270C |
1.075-1.080 |
5 |
Acid Number, Min. |
155-160 |
6 |
Saponification Number, Minimum |
160-165 |
7 |
Volatile matter percent by mass, Max |
1.0 -2.000 |
8 |
Ash content, percent by mass Max |
0.3 -1.000 |
9 |
Matter insolvable in toluene, percent by
mass,Max |
0.6 -2.00 |
10 |
Unsponifiable matter, percent by mass, Max |
4 - 7.8 |
|
1)
The rosin is obtained from Pinus roxburghii ( Chir pine). |
2)
The rosin is obtained by Olustee Process |
3)
The testing has been done by the process defined as per IS:553:1984( except B Grade) |
4)
The product ( except X and B Grade) has been BIS certified vide licence no. 9099801 | |
X - Extra White, WW – Water White, WG –
Window Glass, N–Nancy, M – Mary, K – Kitty, H – Harry, D – Dark & B – Black.
USES |
Paper Sizing, printing inks, protective coatings, adhesives, varnishes and lacquers, grinding and dispersion
of pigments, plasticiser & tackifier in rubber and chewing gums. | |
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